Methanol → HCID 89822875, compound

Participants

Reaction Steps

To a solution of D6 (8 g, 45.6 mmol) in THF (250 mL) cooled at 0° C., BH3 1M in THF (66 mL, 66 mmol) was added and the mixture was stirred at room temperature for 2 hours. Methanol was added, the solution was concentrated in vacuum and co-evaporated twice from methanol to give the title compound as 1/1 diasteroisomeric mixture. Yield (7.6 g, 100%)

Provenance & Evidence