HRID70606

反应详情

EQUATION

反应方程式

HRID 70606 的结构方程式

PROCEDURE

实验过程

The title compound was obtained as a pale yellow solid (3.2 mg, 1% (three steps)) by performing substantially the same reaction as in Examples 1-47(1), 1-2 and 1-1(2) sequentially except for using [4-(cyclopropylsulfanyl)phenyl](6-methoxy-5-methylpyridin-2-yl)methanone obtained in Reference Example 1-37 and using 5-({[1-({[tert-butyl(dimethyl)silyl]oxy}methyl)cyclopropyl]methyl}sulfonyl)-1-phenyl-1H-tetrazole obtained in Reference Example 3-13 in place of 1-phenyl-5-[(tetrahydrofuran-3-ylmethyl)sulfonyl]-1H-tetrazole.

WORKUP

后处理

  1. customthe same reaction as in Examples 1-47(1), 1-2 and 1-1(2) sequentially except
  2. customobtained in Reference Example 1-37