HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → HCID 178517951, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | 5-Aminobenzimidazole | HCID 13623 | — |
| Reactant | Ethyl orthoformate | HCID 31214 | — |
| Reactant | Trimethylsilyl cyanide | HCID 82115 | — |
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 178517951 | HCID 178517951 | — |
Reaction Steps
The compound was synthesized starting from 5-aminobenzimidazole (0.75 g, 5.61 mmol), benzaldehyde (0.52 mL, 5.1 mmol), TMSCN (0.64 mL, 5.1 mmol), conc. aqueous HCl (10 mL), triethyl orthoformate (13 mL, excess), NaBH4 (0.227 g, 6 mmol) as described in method 4.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09173885B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-9eddc4be40cd4254b7c972d71ffc14a1 |
| Source note | uspto-grants-2015_11 |