HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Diaminocyclohexane → HCID 178519152, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Diaminocyclohexane | HCID 4610 | — |
| Reactant | Cesium fluoride | HCID 25953 | — |
| Reactant | Ethyl orthoformate | HCID 31214 | — |
| Reactant | (S)-4-Benzyl-2-oxazolidinone | HCID 736225 | — |
| Reactant | 4-Iodobenzene-1,2-diamine | HCID 11207049 | — |
| Catalyst | Copper(1+) iodide; Copper(I) iodide; Cuprous iodide; Cuprous iodide (CuI) | HCID 24350 | — |
| Product | HCID 178519152 | HCID 178519152 | — |
Reaction Steps
The compound was synthesized starting from (S)-4-benzyloxazolidin-2-one (0.089 g, 0.5 mmol), 4-iodobenzene-1,2-diamine (0.117 g, 0.5 mmol), copper(I) iodide (0.010 g, 0.05 mmol), cesium fluoride (0.276 g, 1 mmol), cyclohexane-1,2-diamine (0.006 mL, 0.05 mmol), triethyl orthoformate (3 mL) as described in method 5 step D.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09173885B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-5f3b79421db94549af526b20ddb24f04 |
| Source note | uspto-grants-2015_11 |