HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → HCID 178516930, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | Thioglycolic Acid | HCID 1133 | — |
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | 5-Aminobenzimidazole | HCID 13623 | — |
| Product | HCID 178516930 | HCID 178516930 | — |
Reaction Steps
The compound was synthesized starting from 5-aminobenzimidazole (0.133 g, 1.0 mmol), benzaldehyde (0.306 mL, 3.0 mmol), mercapto acetic acid (0.276 g, 2.0 mmol), piperidine, according to method 9 step A. yield: 118 mg (40%), MS m/z: 296.3 (M+H)+, HPLC [A]): rt 5.72 min (96%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09173885B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-eb6e72b5000f4bfd9cc9254780c540f9 |
| Source note | uspto-grants-2015_11 |