HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1'-Carbonyldiimidazole → HCID 178517669, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | Trimethylsilyl cyanide | HCID 82115 | — |
| Reactant | 4-Morpholinobenzaldehyde | HCID 291349 | — |
| Reactant | HCID 178507353 | HCID 178507353 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 178517669 | HCID 178517669 | — |
Reaction Steps
The compound was synthesized starting from 1H-benzo[d]imidazol-5-amine (0.333 g, 2.5 mmol), 4-morpholinobenzaldehyde (0.473 g, 2.5 mmol), TMSCN (0.375 mL, 3 mmol), Pd/C (10%, 0.02 g), TEA 1 mL, 7.2 mmol), di-(imidazol-1-yl)methanone (0.600 g, 3.7 mmol) as described in method 2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09173885B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-6bbaeab559bd4d9eb3ffce1d09912206 |
| Source note | uspto-grants-2015_11 |