HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 10943115, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 1'-Hydroxyestragole | HCID 40003 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 10943115 | HCID 10943115 | 100% |
Reaction Steps
To a solution of the allylic alcohol obtained in step 1 (200 mg) in diethyl ether (3 ml) was added thionyl chloride (0.087 ml) and the solution was stirred at room temperature for 1 h. The solution was concentrated in vacuo to give 221 mg of the desired product (100%) as a colorless solid. Mp=70° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09174987B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-c90779fdce8d4dd68aa5393048011391 |
| Source note | uspto-grants-2015_11 |