HuagongsheHuagongshe Chemistry Print Report · For research reference only
Imidazo(1,2-a)pyridine-3-carboxylic acid → 3-Methyl-1-[(6-methylpyridin-3-yl)methyl]-1H-indazol-4-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Imidazo(1,2-a)pyridine-3-carboxylic acid | HCID 73142 | — |
| Reactant | HCID 67974138 | HCID 67974138 | — |
| Product | 3-Methyl-1-[(6-methylpyridin-3-yl)methyl]-1H-indazol-4-amine | HCID 67259803 | 11% |
Reaction Steps
Prepared according to the method of Example 80, replacing 7-(2-methoxyethoxy)imidazo[1,2-a]pyridine-3-carboxylic acid and 1-benzyl-3-methyl-1H-indazol-4-amine with imidazo[1,2-a]pyridine-3-carboxylic acid and 3-methyl-1-((6-methylpyridin-3-yl)methyl)-1H-indazol-4-amine (8 mg, 11% yield). MS (APCI) m/z=397 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09174981B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-8c1be5798b8d4cbcbb2686abdd9eb6e0 |
| Source note | uspto-grants-2015_11 |