HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 178514732, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 4-Fluoro-3-nitrobenzenesulfonamide | HCID 16782487 | — |
| Reactant | HCID 178511581 | HCID 178511581 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178514732 | HCID 178514732 | — |
Reaction Steps
A solution of EXAMPLE 39B (0.40 g), 4-fluoro-3-nitrobenzenesulfonamide (0.478 g) and triethylamine (2 mL) in tetrahydrofuran (10 mL) was stirred for 3 days at room temperature. The reaction mixture was concentrated and purified by flash chromatography (silica gel, 0-30% methanol/dichloromethane) providing the product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09174982B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-38de0691e62a496ab912c44c568dde4b |
| Source note | uspto-grants-2015_11 |