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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 707147Generated: October 29, 2026

Glycinamide hydrochloride → HCID 44546768, compound

https://huagongshe.com/reaction/707147

Reaction equation

Participants

RoleNameHCIDCharge
ReactantGlycinamide hydrochlorideHCID 2723639—
ReactantHCID 86636772HCID 86636772—
CatalystTriethylamineHCID 8471—
ProductHCID 44546768HCID 44546768—

Reaction Steps

Starting from 1-(4-(4-(8-oxa-3-azabicyclo[3.2.1]octan-3-yl)-6-(4-oxopiperidin-1-yl)-1,3,5-triazin-2-yl)phenyl)-3-(pyridin-4-yl)urea-TFA (50 mg) and glycinamide hydrochloride (18 mg) and triethylamine (10 drops) and following the procedure as outlined in example 118 the title compound was isolated as its di-TFA salt after HPLC purification; MS (ES+) 559.8 (M+H)+

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09174963B2
Source datasetuspto-grants-2015_11
ORD IDord-4f7bb853ed754e7caa40072b37bdd2c9
Source noteuspto-grants-2015_11