HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methyl-1-[4-(tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]urea → 1-(4-(4-Chloro-6-(3,5-dimethylmorpholino)-1,3,5-triazin-2-yl)phenyl)-3-methylurea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methyl-1-[4-(tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]urea | HCID 17750273 | — |
| Reactant | 4-(4,6-Dichloro-1,3,5-triazin-2-yl)-3,5-dimethylmorpholine | HCID 86636525 | — |
| Product | 1-(4-(4-Chloro-6-(3,5-dimethylmorpholino)-1,3,5-triazin-2-yl)phenyl)-3-methylurea | HCID 86636524 | 16% |
Reaction Steps
The title compound was prepared by following the procedure of example 462 step 4 using 4-(4,6-dichloro-1,3,5-triazin-2-yl)-3,5-dimethylmorpholine and 1-methyl-3-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-urea. Yield 1.15 g, 16% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09174963B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-5d0a104dafee437bb758fc931a10fb78 |
| Source note | uspto-grants-2015_11 |