Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Propyl Acetate | HCID 7997 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22155088 | HCID 22155088 | — |
Reaction Steps
The dried high DS starch hexanoate described above (Ex. 12, 71.3 g), ethanol (65.2 g), and n-propyl acetate (65.2 g) were charged to a 500 mL round bottom flask, equipped with condenser, overhead stirrer, nitrogen blanket, thermocouple and heating mantle. The mixture was heated to 60° C. for about 1 hr. to form a transparent, low viscosity solution at 30 wt % solids in 50/50 ethanol/n-propyl acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09175179B2 |
|---|
| Source dataset | uspto-grants-2015_11 |
|---|
| ORD ID | ord-ba198b69b5fb4b6aaa592aab49863e33 |
|---|
| Source note | uspto-grants-2015_11 |
|---|