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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 707916Generated: October 30, 2026

3,3-Dimethylpiperidine → HCID 58203725, compound

https://huagongshe.com/reaction/707916

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3,3-DimethylpiperidineHCID 70942—
Reactant8-(1H-Pyrazol-4-yl)-4,5-dihydro-6-oxa-3-thia-1-aza-benzo[e]azulene-2-carboxylic acidHCID 58203883—
ProductHCID 58203725HCID 58203725—

Reaction Steps

Following the procedure for 103, 8-(1H-Pyrazol-4-yl)-4,5-dihydro-6-oxa-3-thia-1-aza-benzo[e]azulene-2-carboxylic acid (50.0 mg, 0.2 mmol) was reacted with 3,3-dimethylpiperidine (1.2 equiv) to give 164 (12.1 mg, M+1 409.1)

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09175009B2
Source datasetuspto-grants-2015_11
ORD IDord-43dd06498fd44026b117ceec37b6d2af
Source noteuspto-grants-2015_11