HRID708023

反应详情

EQUATION

反应方程式

REACTANTS

反应物

反应SMILES：Cc1nc(N)ncc1B1OC(C)(C)C(C)(C)O1

HCID52987906

4-Methyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyrimidin-2-amine

C11H18BN3O2

反应SMILES：CC(C)N(CCO)C(=O)c1nc2c(s1)CCOc1ccc(Br)cc1-2

HCID58204002

未命名化合物

PRODUCTS

产物

反应SMILES：Cc1nc(N)ncc1-c1ccc2c(c1)-c1nc(C(=O)N(CCO)C(C)C)sc1CCO2

HCID58204065

未命名化合物

收率 1.1%

PROCEDURE

实验过程

Following the procedure for 277, 9-Bromo-4,5-dihydro-6-oxa-3-thia-1-aza-benzo[e]azulene-2-carboxylic acid (2-hydroxy-ethyl)-isopropyl-amide (52.2 mg, 0.127 mmol) and 4-methyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyrimidin-2-amine (35.8 mg, 0.152 mmol) were reacted to give 278 (0.6 mg, 1% yield M+1 440.1)

WORKUP

后处理

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