HRID708024

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID2756555

5-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)pyridin-2-amine

C11H17BN2O2

结构：CC(C)N(CCO)C(=O)c1nc2c(s1)CCOc1ccc(Br)cc1-2

HCID58204002

未命名化合物

PRODUCTS

生成物

结构：CC(C)N(CCO)C(=O)c1nc2c(s1)CCOc1ccc(-c3ccc(N)nc3)cc1-2

HCID58203975

未命名化合物

收率 13.3%

PROCEDURE

实验过程

Following the procedure for 277, 9-Bromo-4,5-dihydro-6-oxa-3-thia-1-aza-benzo[e]azulene-2-carboxylic acid (2-hydroxy-ethyl)-isopropyl-amide (52.5 mg, 0.128 mmol) and 5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridin-2-amine (33.7 mg, 0.153 mmol) were reacted to give 279 (7.2 mg, 13% yield, M+1 425.1).

WORKUP

后处理

customwere reacted