HRID708027

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CN(C(=O)OC(C)(C)C)c1ccc(B2OC(C)(C)C(C)(C)O2)cn1

HCID44541676

tert-Butyl methyl[5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridin-2-yl]carbamate

C17H27BN2O4

结构：CC(C)N(CCO)C(=O)c1nc2c(s1)CCOc1ccc(Br)cc1-2

HCID58204002

未命名化合物

PRODUCTS

生成物

结构：CNc1ccc(-c2ccc3c(c2)-c2nc(C(=O)N(CCO)C(C)C)sc2CCO3)cn1

HCID58204273

未命名化合物

收率 2.5%

PROCEDURE

实验过程

Following the procedure for 277, 9-Bromo-4,5-dihydro-6-oxa-3-thia-1-aza-benzo[e]azulene-2-carboxylic acid (2-hydroxy-ethyl)-isopropyl-amide (52.9 mg, 0.129 mmol) and tert-butyl methyl(5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine-2-yl)carbamate (51.6 mg, 0.154 mmol) were reacted to give 282, purified by HPLC (1.4 mg, 2.5% yield, M+1 439.1).

WORKUP

后处理

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