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HRID708118

反应详情

EQUATION

反应方程式

HRID 708118 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(O)Cn1cc(B2OC(C)(C)C(C)(C)O2)cn1
HCID58204131

2-methyl-1-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazol-1-yl]propan-2-ol

C13H23BN2O3

结构：CC(C)n1ncnc1-c1nc2c(s1)CCOc1cc(Br)ccc1-2
HCID66886748

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)n1ncnc1-c1nc2c(s1)CCOc1cc(-c3cnn(CC(C)(C)O)c3)ccc1-2
HCID58203785

未命名化合物

PROCEDURE

实验过程

Similar to as described in General Procedure C, 8-Bromo-2-(2-isopropyl-2H-[1,2,4]triazol-3-yl)-4,5-dihydro-6-oxa-3-thia-1-aza-benzo[e]azulene 27 was reacted with 2-methyl-1-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazol-1-yl)propan-2-ol. Purification of the crude reaction mixture by reverse phase HPLC gave 367. LCMS: 451.1

WORKUP

后处理

  1. customPurification of the crude
  2. customreaction mixture by reverse phase HPLC