Lithium Hydroxide → HCID 118093014, compound

Participants

Reaction Steps

To a solution of 13G (62 mg, 0.075 mmol) in THF (2 mL) was added LiOH (2 mL, 2.000 mmol). The reaction mixture was stirred at rt for 2 days, concentrated and acidified with 1N HCl. The mixture was extracted with EtOAc, washed with brine, dried over Na2SO4, concentrated to give 13H (60 mg, 98% yield).

Provenance & Evidence