HCID 131733871, compound → HCID 123445604, compound

Participants

Reaction Steps

To a solution of 21F (92 mg, 0.173 mmol) in MeOH (5 mL) was added 10% Pd—C (50 mg, 0.047 mmol). The mixture was evacuated and flushed with H2 (3×), then was stirred under a balloon of H2 for 5 h. The mixture was filtered and concentrated to give 21G (62 mg, 0.168 mmol, 97% yield). MS (ESI) m/z: 369.4 (M+H)+.

Provenance & Evidence