HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 131733874, compound → HCID 131733875, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 131733874 | HCID 131733874 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 131733875 | HCID 131733875 | 100% |
Reaction Steps
To 27F (138 mg, 0.372 mmol, 93% yield) in MeOH (5 mL) was added 10% Pd/C (50 mg) and the mixture was hydrogenated (1 atm) for 4 h at rt. The mixture was filtered and concentrated to give 27G (138 mg, 0.372 mmol, 93% yield) as a colorless oil. MS (ESI) m/z: 371.4 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09174974B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-93b4d76611834ded88671c7b70a63c29 |
| Source note | uspto-grants-2015_11 |