HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Trifluoromethoxy)phenylboronic acid → HCID 57824456, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Trifluoromethoxy)phenylboronic acid | HCID 2734386 | — |
| Reactant | HCID 57824452 | HCID 57824452 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 57824456 | HCID 57824456 | — |
Reaction Steps
The compound was prepared by palladium-catalyzed arylation of the product of Step 1 with 4-trifluoromethoxyphenyl boronic acid: 1H NMR (400 MHz, CDCl3) δ 10.14 (s, 1H), 8.91 (d, J=4.2 Hz, 1H), 8.63 (d, J=8.5 Hz, 2H), 8.37 (d, J=8.4 Hz, 2H), 8.06 (d, J=8.8 Hz, 2H), 7.67 (d, J=5.4 Hz, 1H), 7.35 (d, J=8.7 Hz, 2H); EIMS m/z 344 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09179681B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-a9b0b91099d84d599639eacc86c7ab2a |
| Source note | uspto-grants-2015_11 |