4-Methyloxybenzyl chloride → HCID 86731536, compound

HRID 709041Notes

Reaction equation

HRID 709041 reaction equation
C([C:3]1[CH:24]=[CH:23][C:6]([CH2:7][S:8][C:9]2[CH:10]=[C:11]([O:19][CH2:20][O:21][CH3:22])[C:12](=[O:18])[N:13]([CH2:15][O:16][CH3:17])[CH:14]=2)=[CH:5][CH:4]=1)C.ClCC1C=C[C:30]([O:33]C)=CC=1>>[CH3:30][O:33][C:3]1[CH:4]=[CH:5][C:6]([CH2:7][S:8][C:9]2[CH:10]=[C:11]([O:19][CH2:20][O:21][CH3:22])[C:12](=[O:18])[N:13]([CH2:15][O:16][CH3:17])[CH:14]=2)=[CH:23][CH:24]=1

Participants

3

Reactant 2

HCID 699934-Methyloxybenzyl chlorideHCID 867315275-[(4-ethylbenzyl)sulfanyl]-3-(methoxymethoxy)-1-(methoxymethyl)pyridin-2(1H)-one2×

Product 1

HCID 86731536HCID 86731536, compound

Procedure

Prepared as described for 5-[(4-ethylbenzyl)sulfanyl]-3-(methoxymethoxy)-1-(methoxymethyl)pyridin-2(1H)-one (Intermediate 17) but using 1-(chloromethyl)-4-methoxybenzene instead of 1-(chloromethyl)-4-ethylbenzene.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-32265aaf466843648a2d82570c60cf4d
Source dataset
uspto-grants-2015_11
Patent number
US09180122B2

Reaction notes

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