HCID 71187166, compound → HCID 71187313, compound

HRID 709075Notes

Reaction equation

HRID 709075 reaction equation
C(SC1C=C(O)C(=O)NC=1)C1C=CC=CC=1.[CH3:17][O:18][C:19]1[CH:40]=[CH:39][C:22]([CH2:23][S:24][C:25]2[CH:26]=[C:27]([O:35]COC)[C:28](=[O:34])[N:29](COC)[CH:30]=2)=[CH:21][CH:20]=1>>[OH:35][C:27]1[C:28](=[O:34])[NH:29][CH:30]=[C:25]([S:24][CH2:23][C:22]2[CH:39]=[CH:40][C:19]([O:18][CH3:17])=[CH:20][CH:21]=2)[CH:26]=1

Participants

3

Reactant 2

HCID 71187166HCID 71187166, compoundHCID 86731536HCID 86731536, compound2×

Product 1

HCID 71187313HCID 71187313, compound

Procedure

Prepared as described for 5-(benzylsulfanyl)-3-hydroxypyridin-2(1H)-one (Example 12) from 5-[(4-methoxybenzyl)sulfanyl]-3-(methoxymethoxy)-1-(methoxymethyl)pyridin-2(1H)-one (Intermediate 26).

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-0f950721aca6460ca820d4b7ee73fc79
Source dataset
uspto-grants-2015_11
Patent number
US09180122B2

Reaction notes

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