HCID 71187166, compound → HCID 71187148, compound

HRID 709079Notes

Reaction equation

HRID 709079 reaction equation
C(SC1C=C(O)C(=O)NC=1)C1C=CC=CC=1.COC[O:20][C:21]1[C:22](=[O:40])[N:23](COC)[CH:24]=[C:25]([S:27][CH2:28][C:29]2[CH:30]=[N:31][C:32]([O:35][CH3:36])=[CH:33][CH:34]=2)[CH:26]=1>>[OH:20][C:21]1[C:22](=[O:40])[NH:23][CH:24]=[C:25]([S:27][CH2:28][C:29]2[CH:30]=[N:31][C:32]([O:35][CH3:36])=[CH:33][CH:34]=2)[CH:26]=1

Participants

3

Reactant 2

HCID 71187166HCID 71187166, compoundHCID 86731540HCID 86731540, compound2×

Product 1

HCID 71187148HCID 71187148, compound

Procedure

Prepared as described for 5-(benzylsulfanyl)-3-hydroxypyridin-2(1H)-one (Example 12) from 3-(methoxymethoxy)-1-(methoxymethyl)-5-{[(6-methoxypyridin-3-yl)methyl]sulfanyl}pyridin-2(1H)-one (Intermediate 30).

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-83582a0b2a3c4f9086d36038245fe63e
Source dataset
uspto-grants-2015_11
Patent number
US09180122B2

Reaction notes

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