Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Benzylamine | HCID 7504 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | Dibenzylamine | HCID 7656 | 91% |
Reaction Steps
To carry out the oxidative condensation, benzylamine (0.5 mmol) was heated with catalyst Pd@ba-GO (10 mg) and solvent CH3CN (0.2 mL) at 90° C. in a flask open to air for 6 hours, and then stirred also at 90° C. under H2 gas (1 atm) for 6 hours to obtain dibenzylamine. An unexpectedly high yield of 91% was achieved.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09180442B2 |
|---|
| Source dataset | uspto-grants-2015_11 |
|---|
| ORD ID | ord-93f19989abb9418cacc99c520cf99ffe |
|---|
| Source note | uspto-grants-2015_11 |
|---|