HCID 178477811, compound → 2-Amino-3-(4,6-dibromo-5,7-dichloro-2H-benzotriazol-2-yl)-2-methylpropionitrile

HRID 70959Notes

Reaction equation

HRID 70959 reaction equation
[Br:1][C:2]1[C:10]2[N:9]=[N:8][NH:7][C:6]=2[C:5]([Cl:11])=[C:4]([Br:12])[C:3]=1[Cl:13].Br[C:15]1[C:23]2[N:22]=N[NH:20][C:19]=2C(Cl)=CC=1Cl.Cl[C:27]1C=C(Cl)C2NN=NC=2C=1>>[NH2:22][C:23]([CH3:15])([CH2:27][N:8]1[N:7]=[C:6]2[C:5]([Cl:11])=[C:4]([Br:12])[C:3]([Cl:13])=[C:2]([Br:1])[C:10]2=[N:9]1)[C:19]#[N:20]

Participants

4

Reactant 3

HCID 178477811HCID 178477811, compoundHCID 178478176HCID 178478176, compoundHCID 178478177HCID 178478177, compound

Product 1

HCID 666201482-Amino-3-(4,6-dibromo-5,7-dichloro-2H-benzotriazol-2-yl)-2-methylpropionitrile

Procedure

2-Amino-3-(4,6-dibromo-5,7-dichloro-2H-benzotriazol-2-yl)-2-methylpropionitrile was prepared using a procedure similar to that described in Example 1, part a and b, except starting from 4,6-dibromo-5,7-dichloro-1H-benzotriazole that was prepared along with 4-bromo-5,7-dichloro-1H-benzotriazole described in Example 55 using a procedure similar to that described in Example 53 except using 5,7-dichloro-1H-benzotriazole described in Example 15.

Sources & evidence

ORD record
ord-c9cc6db37ac342589f5104f6fe612b26
Source dataset
uspto-grants-2014_09
Patent number
US08822689B2

Reaction notes

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