2,3-Dichloropyridine → HCID 47129949, compound

HRID 709594Notes

Reaction equation

HRID 709594 reaction equation
[CH3:1][O:2][C:3](=[O:13])[CH2:4][S:5][C:6]1[CH:11]=[CH:10][C:9](Cl)=[CH:8][N:7]=1.[Cl:14]C1C(Cl)=CC=CN=1>>[CH3:1][O:2][C:3](=[O:13])[CH2:4][S:5][C:6]1[C:11]([Cl:14])=[CH:10][CH:9]=[CH:8][N:7]=1

Participants

3

Reactant 2

HCID 169882,3-DichloropyridineHCID 60735499HCID 60735499, compound

Product 1

HCID 47129949HCID 47129949, compoundYield 52%

Procedure

was synthesized according to the procedure used for compound 14. Starting with 2,3-dichloropyridine (17, 2.09 g, 14.0 mmol) the target 18 was obtained as a colorless oil (1.6 g, 52% yield).

Workup

  1. customwas synthesized

Sources & evidence

ORD record
ord-e326648906194ba999ec0f7bf973f626
Source dataset
uspto-grants-2015_11
Patent number
US09181219B2

Reaction notes

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