2-(2-Methylallyl)propane-1,3-diol → Tetrahydro-5,5-dimethyl-3-furanmethanol

Participants

Reaction Steps

Under a nitrogen atmosphere, a solution of 2-(2-methylallyl)propane-1,3-diol (2.00 g) and silver trifluoromethanesulfonate (197 mg) in dichloromethane (40 mL) was stirred at 80° C. for 2 days. The reaction mixture was filtered through celite, and the filtrate was evaporated under reduced pressure to give the title compound (2.00 g) as a brown oil. This compound was used for the next step without further purification.

Provenance & Evidence