HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 1-Amino-3-(3,4-dimethoxyphenoxy)propan-2-one hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1-(3,4-Dimethoxyphenoxy)-3-nitropropan-2-one | HCID 86706774 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 1-Amino-3-(3,4-dimethoxyphenoxy)propan-2-one hydrochloride | HCID 86706775 | — |
Reaction Steps
To a MeOH (7 ml) solution of the compound (0.660 g) obtained in Example 19-(2), 10% Pd—C (0.330 g) and an aqueous solution of 1N HCl (14 ml) were added and the mixture was stirred at room temperature for 5 hours in a hydrogen gas atmosphere. The insoluble matter was filtered off and the filtrate was concentrated to give the titled compound (0.715 g, brown amorphous.)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09181229B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-0343177e56eb4de2aea60c267dd6a7c7 |
| Source note | uspto-grants-2015_11 |