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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 710086Generated: October 30, 2026

HCID 71089559, compound → HCID 71089548, compound

https://huagongshe.com/reaction/710086

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 71089559HCID 71089559—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 71089548HCID 71089548102.5%

Reaction Steps

Intermediate 24 (100 mg, 0.23 mmol) dissolved in MeOH (10 ml) and added Pd/C (100 mg). This mixture was stirred under 60 Psi hydrogen atmosphere in an autoclave for 16. After 16 h, reaction mass filtered through celite and celite was washed with MeOH. MeOH was removed on rotavapour to obtain the titled compound (80 mg) as an off-white solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09181214B2
Source datasetuspto-grants-2015_11
ORD IDord-dcce5459e5054e0d86ad8360939db9a3
Source noteuspto-grants-2015_11