HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methyl 3-(1-adamantyl)-4-methoxybenzoate → 4-(1-Admantyl)-3-methoxybenzoic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methyl 3-(1-adamantyl)-4-methoxybenzoate | HCID 14549070 | — |
| Edukt | Methyl 4-(1-admantyl)-3-methoxybenzoate | HCID 66726966 | — |
| Produkt | 4-(1-Admantyl)-3-methoxybenzoic acid | HCID 53960528 | 88% |
Reaktionsschritte
When the product of Step A was substituted for methyl-3-(1-admantyl)-4-methoxybenzoate in Example 30, Step B the similar process afforded the title compound in 88% yield. 1H-NMR (CDCl3) 1.7 (s, 6H); 2.01 (s, 3H); 2.06 (s, 6H); 3.81 (s, 3H); 7.19 (d, 1H, J=8.1 Hz); 7.45 (d, 1H, J=1.49 Hz); 7.53 (d, 1H, J=1.61, 8.11 Hz).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09181182B2 |
| Quelldatensatz | uspto-grants-2015_11 |
| ORD ID | ord-294062331c0f40768507cd9880472210 |
| Quellennotiz | uspto-grants-2015_11 |