HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(3,4-Diethoxyphenyl)-3-(1H-indol-4-yl)-1,2,4-oxadiazole → HCID 66726622, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(3,4-Diethoxyphenyl)-3-(1H-indol-4-yl)-1,2,4-oxadiazole | HCID 25110297 | — |
| Reactant | HCID 66726256 | HCID 66726256 | — |
| Product | HCID 66726622 | HCID 66726622 | 95% |
Reaction Steps
When the product of Step C was substituted for 5-(3,4-diethoxyphenyl)-3-(1H-indol-4-yl)-1,2,4-oxadiazole in Example 34, Step C, the identical process afforded the title compound in 95% yield. 1H-NMR (CDCl3) 1.10 (tr, 3H, J=7.38 Hz); 1.85-1.94 (m, 2H); 3.54 (tr, 2H, J=7.92 Hz); 3.75 (tr, 2H, J=8.28 Hz); 4.08 (tr, 2H, J=6.42 Hz); 6.98 (d, 1H, J=8.73 Hz); 7.03 (d, 1H, J=7.77 Hz); 7.26 (tr, 1H, J=7.83 Hz); 7.75 (d, 1H, J=7.17 Hz); 8.09 (dd, 1H, J=2.1, 8.61 Hz); 8.39 (d, 1H, J=2.1 Hz).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09181182B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-5f60cedaac6149708fa68436c92e43a5 |
| Source note | uspto-grants-2015_11 |