4-Chlorobenzylamine → HCID 178478133, compound

HRID 710503Notes

Reaction equation

HRID 710503 reaction equation
O1[CH:5]=[N:4][N:3]=[C:2]1[C:6]1[CH:14]=[CH:13][C:9]2[N:10]=[CH:11][NH:12][C:8]=2[CH:7]=1.[Cl:15][C:16]1[CH:23]=[CH:22][C:19]([CH2:20][NH2:21])=[CH:18][CH:17]=1>>[Cl:15][C:16]1[CH:23]=[CH:22][C:19]([CH2:20][N:21]2[CH:5]=[N:4][N:3]=[C:2]2[C:6]2[CH:14]=[CH:13][C:9]3[NH:10][CH:11]=[N:12][C:8]=3[CH:7]=2)=[CH:18][CH:17]=1

Participants

3

Reactant 2

HCID 660364-ChlorobenzylamineHCID 58433284HCID 58433284, compound

Product 1

HCID 178478133HCID 178478133, compound

Procedure

The compound was synthesized starting from 5-(1,3,4-oxadiazol-2-yl)benzimidazole (186 mg, 1 mmol) and 4-chlorobenzylamine (0.5 ml) as described above; yield: 0.063 g (20.4%);

Workup

  1. customThe compound was synthesized

Sources & evidence

ORD record
ord-caea8daadb6c4ac69debbbb96b5b42db
Source dataset
uspto-grants-2015_11
Patent number
US09181233B2

Reaction notes

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