HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxychloride → HCID 178478072, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | Lawesson's reagent | HCID 87949 | — |
| Reactant | 3-(2,4-Dichlorophenyl)propanoic acid | HCID 2740915 | — |
| Reactant | 1H-benzimidazole-5-carbohydrazide | HCID 16637119 | — |
| Product | HCID 178478072 | HCID 178478072 | — |
Reaction Steps
The compound was synthesized starting from 3-(2,4-dichlorophenyl)propionic acid (220 mg; 1 mmol), benzimidazol-5-carbohydrazide (176 mg; 1 mmol), Lawesson's reagent (606 mg; 1.5 mmol) and POCl3 (0.137 ml; 1.5 mmol) as described in method 3; yield: 0.016 g (4.3%);
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09181233B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-54b7f1cd933f44a5ace207c066cc7149 |
| Source note | uspto-grants-2015_11 |