Benzyl isocyanate → HCID 178518788, compound

Participants

Reaction Steps

The compound was synthesized starting from benzimidazol-5-carbohydrazide (176 mg; 1 mmol) and benzylisocyanate (0.133 g; 0.123 ml; 1 mmol); Yield: 0.077 (26%); MS m/z: 292.4 [M+H]+; 1H-NMR (DMSO d6, 400 MHz): δ 4.92 (s, 2H); 7.02-7.04 (m, 2H); 7.23-7.27 (m, 3H); 7.52 (dd, 1H, 4J=1.7 Hz, 3J=8.7 Hz); 7.76 (d, 1H, 3J=8.7 Hz); 7.81 (m, 1H); 8.99 (s, 1H), 12.08 (s, 1H); HPLC (METHOD [A]): rt 8.28 min (100%)

Provenance & Evidence