Benzyl Isothiocyanate → HCID 178527912, compound

Participants

Reaction Steps

The compound was synthesized starting from benzimidazol-5-carbohydrazide (176 mg; 1 mmol) and benzylisothiocyanate (0.149 g; 0.13 ml; 1 mmol); Yield: 0.052 g (17%); MS m/z: 308.3 [M+H]+; 1H-NMR (DMSO d6, 400 MHz): δ 5.33 (s, 2H); 6.97-6.99 (m, 2H); 7.15-7.22 (m, 3H); 7.44 (dd, 1H, 4J=1.7 Hz, 3J=8.7 Hz); 7.71 (d, 1H, 3J=8.7 Hz), 7.81 (br s, 1H); 8.79 (s, 1H); 14.08 (s, 1H); HPLC (METHOD [A]): rt 10.47 min (100%)

Provenance & Evidence