HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridinium chloride → HCID 58220015, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridinium chloride | HCID 10176127 | — |
| Reactant | 2,11-Dimethoxytriphenylene | HCID 58220008 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 58220015 | HCID 58220015 | 94% |
Reaction Conditions
| Temperature | 220 °C |
|---|
Reaction Steps
A mixture of 2,11-dimethoxytriphenylene (8.8 g, 30.5 mmol) and pyridine hydrochloride (31.73 g, 274.6 mmol) was heated to 220° C. for 2 hours. The mixture was cooled and water was added. The resulting solid was filtered off, washed with water, and dried under high vacuum. 7.45 g (94%) desired product was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08822708B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-985b906909b041b78d92db7ff246cff7 |
| Source note | uspto-grants-2014_09 |