HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Furancarboxylic acid, hydrazide → HCID 117988348, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Furancarboxylic acid, hydrazide | HCID 18731 | — |
| Reactant | (2S,5R)-6-(Benzyloxy)-7-oxo-1,6-diazabicyclo[3.2.1]octane-2-carboxylic acid | HCID 57389355 | — |
| Product | HCID 117988348 | HCID 117988348 | 37.9% |
Reaction Steps
Following a procedure analogous to Example 27, from the carboxylic acid (6b, 552 mg, 2.00 mmol) of Example 9 or 16 and furan-2-carbohydrazide (390 mg, prepared following a procedure analogous to Reference Example 6 from the compound described in Reference Example 3), 291.8 mg of the title compound was afforded (yield 37.9%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09181250B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-b5080bf334374de58c2db51c682bbc80 |
| Source note | uspto-grants-2015_11 |