Ethylenediamine → Benzyl N-(2-aminoethyl)carbamate

Participants

Reaction Conditions

Reaction Steps

A solution of benzylchloroformate (1.3 mL, 9 mmol) in DCM (25 mL) was added over 1.5 h to a solution of 1,2-diaminoethane (6 mL, 90 mmol) in DCM (95 mL) cooled at 0° C. The solution was stirred for 2 h at 0° C., then the solution was washed with brine (40 mL).

Provenance & Evidence