HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromine → HCID 178516705, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | HCID 178516710 | HCID 178516710 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 178516705 | HCID 178516705 | 90% |
Reaction Steps
Bromine (0.895 mL, 15.5 mmol) was added to the solution of quinoxalin-2-ol (1.5 g, 10.3 mmol) in HOAc (15 mL), the mixture was stirred at r.t. for 6 h, and the precipitate was collected and washed with ethyl ether and dried to afford 7-bromoquinoxalin-2-ol as a solid in 90% yield (2 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09181264B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-f19a51d543424f9b8ea1bc10a8a907b6 |
| Source note | uspto-grants-2015_11 |