HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl isocyanate → N-(2-Cyano-5-methylphenylcarbamoyl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl isocyanate | HCID 78210 | — |
| Reactant | 2-Amino-4-methylbenzonitrile | HCID 2801276 | — |
| Product | N-(2-Cyano-5-methylphenylcarbamoyl)benzamide | HCID 57456915 | — |
Reaction Steps
Prepared as in Example 1a from 2-amino-4-methylbenzonitrile and benzoyl isocyanate as a white solid. 1H NMR (400 MHz, DMSO-d6) δ 7.10-7.13 (m, 1H), 7.54 (t, J=7.8 Hz, 2H), 7.66 (t, J=7.8 Hz, 1H), 7.71 (d, J=8.0 Hz, 1H), 8.02-8.04 (m, 2H), 8.07 (s, 1H), 11.32 (s, 1H), 11.44 (s, 1H). MS 280 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09181276B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-41e2b8790be24c8789c60a48ffc1efdb |
| Source note | uspto-grants-2015_11 |