HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → 2-chloro-N-methylquinazolin-4-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | 2,4-Dichloroquinazoline | HCID 252886 | — |
| Product | 2-chloro-N-methylquinazolin-4-amine | HCID 318057 | — |
Reaction Steps
Prepared as in Example 38 from 2,4-dichloroquinazoline and methylamine. 1H NMR (400 MHz, DMSO-d6) δ 2.98 (d, J=4.4 Hz, 3H), 7.53-7.49 (m, 1H), 7.61-7.58 (m, 1H), 7.79-7.75 (m, 1H), 88.19-8.17 (m, 1H), 0.78 (bs, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09181276B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-3d6686c2269f4c0d8acf08ba439a2150 |
| Source note | uspto-grants-2015_11 |