HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl isocyanate → N-(2-cyano-5-hydroxyphenylcarbamoyl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl isocyanate | HCID 78210 | — |
| Reactant | 2-Amino-4-hydroxybenzonitrile | HCID 12468683 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | N-(2-cyano-5-hydroxyphenylcarbamoyl)benzamide | HCID 57456929 | — |
Reaction Steps
Prepared as in Example 53a, but refluxed in acetone instead of 1,4-dioxane, from 2-amino-4-hydroxybenzonitrile and benzoyl isocyanate as a yellow solid (399 mg, 94%). MS 281 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09181276B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-95edcff2d521480cbb2988182ce45161 |
| Source note | uspto-grants-2015_11 |