HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorosulfamic acid → N-(2-cyano-4-chlorophenyl)sulfamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorosulfamic acid | HCID 24499 | — |
| Reactant | 2-Amino-5-chlorobenzonitrile | HCID 80019 | — |
| Product | N-(2-cyano-4-chlorophenyl)sulfamide | HCID 67399964 | — |
Reaction Steps
Prepared as in Example 77a from 2-amino-5-chlorobenzonitrile and sulfamoyl chloride. 1H NMR (400 MHz, DMSO-d6) 7.3 (S, 2H), 7.54-7.56 (d J=9.2 Hz, 1H), 7.74-7.77 (dd J=8.4 Hz, 2 Hz, 1H) 9.67 (s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09181276B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-a5f6846060454393b6fa190b1e3c1d6b |
| Source note | uspto-grants-2015_11 |