Chlorosulfamic acid → HCID 67400359, compound

HRID 711707Notes

Reaction equation

HRID 711707 reaction equation
[NH2:1][C:2]1[CH:9]=[CH:8][CH:7]=[C:6]([S:10][CH3:11])[C:3]=1[C:4]#[N:5].[S:12](Cl)(=[O:15])(=[O:14])[NH2:13]>>[S:12]([NH:1][C:2]1[CH:9]=[CH:8][CH:7]=[C:6]([S:10][CH3:11])[C:3]=1[C:4]#[N:5])(=[O:15])(=[O:14])[NH2:13]

Participants

3

Reactant 2

HCID 24499Chlorosulfamic acidHCID 12715767HCID 12715767, compound

Product 1

HCID 67400359HCID 67400359, compound

Procedure

Prepared as in Example 1 from 2-amino-6-(methylthio)benzonitrile (Example 8b) and sulfamoyl chloride. 1H NMR (400 MHz, DMSO-d6) δ 2.56 (s, 3H), 7.18 (d, J=8.4 Hz, 1H), 7.26 (s, 2H), 7.33 (d, J=8.0 Hz, 1H), 7.59 (t, J=8.40 Hz, 1H), 9.51 (s, 1H).

Sources & evidence

ORD record
ord-e6eb25ab417c4f978de72e80cd396c64
Source dataset
uspto-grants-2015_11
Patent number
US09181276B2

Reaction notes

Loading…