HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → 2-Nitro-6-methylaminobenzonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | Dinitrobenzonitrile | HCID 520718 | — |
| Product | 2-Nitro-6-methylaminobenzonitrile | HCID 12715771 | 79% |
Reaction Steps
Prepared as in Example 90c from 2,6-dinitrobenzonitrile and methylamine to give 2-methylamino-6-nitrobenzonitrile (0.42 g, 79%). 1H NMR (400 MHz, DMSO-d6) δ 2.85 (d, J=5.2 Hz, 3H), 6.75 (d, J=4.8 Hz, NH), 7.16 (d, J=8.4 Hz, 1H), 7.45 (d, J=7.6 Hz, 1H), 7.64 (t, J=8.4 Hz, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09181276B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-f775560aa0a64e8f95892ff94bd4ed6c |
| Source note | uspto-grants-2015_11 |