Benzoyl isocyanate → HCID 67399785, compound

HRID 711834Notes

Reaction equation

HRID 711834 reaction equation
[NH2:1][C:2]1[CH:9]=[CH:8][CH:7]=[C:6]([O:10][CH2:11][C:12]([CH3:15])([CH3:14])[CH3:13])[C:3]=1[C:4]#[N:5].[C:16]([N:24]=[C:25]=[O:26])(=[O:23])[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1>>[C:4]([C:3]1[C:6]([O:10][CH2:11][C:12]([CH3:15])([CH3:14])[CH3:13])=[CH:7][CH:8]=[CH:9][C:2]=1[NH:1][C:25]([NH:24][C:16](=[O:23])[C:17]1[CH:18]=[CH:19][CH:20]=[CH:21][CH:22]=1)=[O:26])#[N:5]

Participants

3

Reactant 2

HCID 78210Benzoyl isocyanateHCID 66745775HCID 66745775, compound

Product 1

HCID 67399785HCID 67399785, compoundYield 96%

Procedure

Prepared as in Example 146a from 2-amino-6-(neopentyloxy)-benzonitrile (Example 217b) and benzoyl isocyanate in 96% yield as a white solid. MS 352 (MH+).

Sources & evidence

ORD record
ord-717ca688f1e74d28971298c341bd59fc
Source dataset
uspto-grants-2015_11
Patent number
US09181276B2

Reaction notes

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