Dinitrobenzonitrile → HCID 66746434, compound

HRID 711841Notes

Reaction equation

HRID 711841 reaction equation
[CH2:1]([NH:5][C:6](=[O:12])[C:7]([CH3:11])([CH3:10])[CH2:8][OH:9])[CH2:2][CH2:3][CH3:4].[N+:13]([C:16]1[CH:23]=[CH:22][CH:21]=[C:20]([N+]([O-])=O)[C:17]=1[C:18]#[N:19])([O-:15])=[O:14]>>[CH2:1]([NH:5][C:6](=[O:12])[C:7]([CH3:11])([CH3:10])[CH2:8][O:9][C:20]1[CH:21]=[CH:22][CH:23]=[C:16]([N+:13]([O-:15])=[O:14])[C:17]=1[C:18]#[N:19])[CH2:2][CH2:3][CH3:4]

Participants

3

Reactant 2

HCID 520718DinitrobenzonitrileHCID 14491555HCID 14491555, compound

Product 1

HCID 66746434HCID 66746434, compoundYield 66%

Procedure

Prepared as in Example 215c from N-butyl-3-hydroxy-2,2-dimethylpropanamide (Example 228c) and 2,6-dinitrobenzonitrile in 66% yield. MS 320 (MH+).

Sources & evidence

ORD record
ord-acb31d0b27b04407aaf03693667abbef
Source dataset
uspto-grants-2015_11
Patent number
US09181276B2

Reaction notes

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