Chlorosulfamic acid → HCID 66747228, compound

HRID 711843Notes

Reaction equation

HRID 711843 reaction equation
[NH2:1][C:2]1[C:3]([C:19]#[N:20])=[C:4]([CH:16]=[CH:17][CH:18]=1)[O:5][CH2:6][C:7]([NH:10][C:11](=[O:15])[CH2:12][CH2:13][CH3:14])([CH3:9])[CH3:8].[S:21](Cl)(=[O:24])(=[O:23])[NH2:22]>>[S:21]([NH:1][C:2]1[C:3]([C:19]#[N:20])=[C:4]([CH:16]=[CH:17][CH:18]=1)[O:5][CH2:6][C:7]([NH:10][C:11](=[O:15])[CH2:12][CH2:13][CH3:14])([CH3:9])[CH3:8])(=[O:24])(=[O:23])[NH2:22]

Participants

3

Reactant 2

HCID 24499Chlorosulfamic acidHCID 66745706HCID 66745706, compound

Product 1

HCID 66747228HCID 66747228, compoundYield 100%

Procedure

Prepared as in Example 215a from N-(1-(3-amino-2-cyanophenoxy)-2-methylpropan-2-yl)butyramide (Example 229b) and sulfamoyl chloride in 100% yield. MS 355 (MH+).

Sources & evidence

ORD record
ord-f8852fac17dd4a33ae30a02dc680d45a
Source dataset
uspto-grants-2015_11
Patent number
US09181276B2

Reaction notes

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