Chlorosulfamic acid → HCID 67399762, compound

HRID 711849Notes

Reaction equation

HRID 711849 reaction equation
[C:1]([O:4][C:5]([CH3:19])([CH2:7][CH2:8][O:9][C:10]1[CH:15]=[CH:14][CH:13]=[C:12]([NH2:16])[C:11]=1[C:17]#[N:18])[CH3:6])(=[O:3])[CH3:2].[S:20](Cl)(=[O:23])(=[O:22])[NH2:21]>>[C:1]([O:4][C:5]([CH3:19])([CH2:7][CH2:8][O:9][C:10]1[CH:15]=[CH:14][CH:13]=[C:12]([NH:16][S:20](=[O:23])(=[O:22])[NH2:21])[C:11]=1[C:17]#[N:18])[CH3:6])(=[O:3])[CH3:2]

Participants

3

Reactant 2

HCID 24499Chlorosulfamic acidHCID 67400400HCID 67400400, compound

Product 1

HCID 67399762HCID 67399762, compoundYield 100%

Procedure

Prepared as in Example 215a from 4-(3-amino-2-cyanophenoxy)-2-methylbutan-2-yl acetate (Example 231b) and sulfamoyl chloride in 100% yield. MS 342 (MH+).

Sources & evidence

ORD record
ord-252d0daf68404e9a944ca4b5f3aa734a
Source dataset
uspto-grants-2015_11
Patent number
US09181276B2

Reaction notes

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